Greener synthesis of 1,2-butylene carbonate from CO2 using graphene-inorganic nanocomposite catalyst

Journal article


Onyenkeadi, V, Kellici, S and Saha, B (2018). Greener synthesis of 1,2-butylene carbonate from CO2 using graphene-inorganic nanocomposite catalyst. Energy. 165, pp. 867-876. https://doi.org/10.1016/j.energy.2018.09.135
AuthorsOnyenkeadi, V, Kellici, S and Saha, B
Abstract

The synthesis of 1,2-butylene carbonate (BC) from cycloaddition reaction of 1,2-butylene oxide (BO) and carbon dioxide (CO2) was investigated using several heterogeneous catalysts in the absence of organic solvent. Continuous hydrothermal flow synthesis (CHFS) has been employed as a rapid and cleaner route for the synthesis of a highly efficient graphene-inorganic heterogeneous catalyst, ceria-lanthana-zirconia/graphene nanocomposite, represented as Ce–La–Zr/GO. The heterogeneous catalysts have been characterised using transmission electron microscopy (TEM), X-ray photoelectron spectroscopy (XPS), X-ray powder diffraction (XRD) and nitrogen adsorption/desorption (BET for measuring the surface area/pore size distribution),. Ceria- lanthana-zirconia/graphene nanocomposite catalyst (Ce–La–Zr/GO) exhibited high catalytic activity as compared to other reported heterogeneous catalysts in the absence of any organic solvent with a selectivity of 76% and 64% yield of 1,2-butylene carbonate at the reaction conditions of 408 K, 75 bar in 20 h.

Keywords0913 Mechanical Engineering; 0915 Interdisciplinary Engineering; Energy
Year2018
JournalEnergy
Journal citation165, pp. 867-876
PublisherElsevier
ISSN0360-5442
Digital Object Identifier (DOI)https://doi.org/10.1016/j.energy.2018.09.135
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Print20 Sep 2018
Publication process dates
Deposited08 Oct 2018
Accepted19 Sep 2018
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